preparation of p-toluenesulfonyl azide_kain industrial additive

background and overview p-toluenesulfonyl azide is a chemical intermediate with a wide range of uses. preparation[1] at room temperature, add 13.8g p-toluenesulfonyl chloride (73mmol), 50ml water and 5.7g sodium azide (87mmol) in sequence in a 500ml flask, stir for 2 hours, and monitor the reaction with tlc until the reaction is complete. extract 3 times…

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